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This article demonstrates a green route for synthesis of Ca‐doped [Mg3Al(OH)8]Cl from a reaction of AlCl3·6H2O, Mg(OH)2, Ca(OH)2, and NH3·H2O in water, which produces only the desired solid product and a by‐product NH4Cl in the mother solution; therefore, they can be separated easily by filtration or centrifugation. Being carefully designed, enough NH4Cl can be crystallized from the mother solution,...
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