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Three metal covalent organic frameworks (MCOFs), namely RuCOF‐ETTA, RuCOF‐TPB and RuCOF‐ETTBA, were synthesized by incorporating the photosensitive RuII tris(2,2′‐bipyridine) unit into the skeleton. Interestingly, each RuCOF contains three isostructural covalent organic frameworks that interlock together with the RuII centers serving as point of registry. The covalently linked network coupling with...
The construction of three‐dimensional (3D) covalent organic frameworks (COFs) remains challenging due to the limited types of organic building blocks. With octahedral TiIV complex as the building unit, this study reports on the first 3D anionic titanium‐based COF (Ti‐COF‐1) with an edge‐transitive (6, 4)‐connected soc topology. Ti‐COF‐1 exhibits high crystallinity, superior stability, and large specific...
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