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Synchrotron radiation is applied to the combined anomalous small angle X-ray scattering (ASAXS) and X-ray absorption near-edge structure (XANES) in situ studies of platinum electrocatalysts, whose metal content is highly dispersed in the form of small crystallites on high surface area porous carbon supports. Combined measurements with X-ray energies near the Pt-L 3 X-ray absorption edge have...
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