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The diffuse scattering from the surfaces of melt and glassy polymer brushes has been studied systematically for the first time using polystyrene (PS) and poly(n-butylacrylate) (PnBA) brushes synthesized by free radical polymerization. The data show unambiguously that the diffuse scattering behavior varies systematically with brush thickness for both types of brushes. We attribute a cross-over in scattering...
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