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The discovery of naturally occurring linker‐based zirconium MOFs with permanent porosity and accessible functional groups remains a challenge. Using trans‐aconitic acid to assemble with Zr6 oxoclusters under green and scalable conditions, a novel microporous Zr‐aconitate framework has been prepared successfully with a high space‐time yield. This MOF is isostructural to the previously reported Zr‐fumarate,...
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