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During heating of nickel acetate solution at a constant rate of 4°C/min up to 350°C, α-type anion-exchangeable layered hydroxide Ni 2 (OH) 3 (OCOCH 3 )1.4H 2 O, containing the acetate anions in the interlayer spaces, first crystallized at 160°C. A second-stage intermediate phase losing the acetate guest in every second layer appeared at 180°C and subsequently transformed...
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