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We report the synthesis of HKUST‐1 (Cu3(btc)2; btc=benzene‐1,3,5‐tricarboxylate) and its growth kinetics by dynamic light scattering completely at room temperature without prior nucleation‐induction steps. Upon an increase in concentration of the starting solutions, the generation of a pure phase requires adjustment of the H2O/EtOH ratio. The presence of DMF is important to avoid competitive side...
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