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6,7-dideoxy-1,2;3,4;9,10-tris-O-(1-methylethylidene)-d-erythro-α-d-galacto-undecopy- ranosid-8-ulose, 3, was formed by adding a D-galactose-derived dithiane nucleophile to a protected erythronolactone followed by reductive removal of the dithioacetal group. Its β-anomer crystallizes in the chiral trigonal space group P3221 with a=b=12.2649(19) Å, c=24.675(8) Å, and Z=6. The molecule is composed of...
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