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Rhenium(III) chloride reacts with sodium isopropylthiolate to give the homoleptic rhenium thiolate cluster Re 3 (μ-SPr i3 (SPr i6 in moderate yield. Proton and 13 C NMR spectra indicate the cluster has virtual C s symmetry in solution due to the high barrier to inversion for the three-coordinate sulfur atoms at the bridging sites. The Re–Re bond distances...
The THF adduct of rhenium trichloride, Re 3 (μ-Cl) 3 Cl 6 (THF) 3 , reacts with trimethylphosphine and NaOPr i to give the chloro-hydride Re 3 (μ-OPr i ) 3 Cl(H)(OPr) i ) 4 (PMe 3 ) and the dimer {Re 3 (μ-OPr i ) 3 Cl(OPr i ) 4 } 2 (μ-Cl) 2 in moderate yields...
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