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Fourier-transform (FT) Raman and near infrared (NIR) spectra have been measured for poly(methyl methacrylate) (PMMA) and its immiscible blends with atactic polystyrene (PS) of small PS contents from 1 to 10 wt.%. Generalized two-dimensional (2D) correlation spectroscopy has been applied to analyze the composition-dependent FT-Raman and NIR spectral variations of the immiscible blends. The synchronous...
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