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Monitoring of unstable intermediates is very important for clarifying complex electrochemical reaction pathways. A combination of thin-layer spectral and electrophoretic electrochemistry, both based on fast thin-layer electrolysis, has been developed to monitor the intermediates of electro-oxidation of clioquinol in acidic, physiological and alkaline buffer media. Two thin-layer electrochemical cells...
This paper describes a novel method of obtaining cyclic voltammograms (CVs) from optical signals. The obtained CVs correspond to the various specific species involved in the electrode process, which give more detailed information on the system under investigation than the common CV. For this purpose cyclic voltabsorptometry was used to investigate the successive oxidation processes of rutin on a graphite-wax...
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