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In this work, the stability of nanoparticles during the dehydration/oligomerization (D/O) stage in situ melt polycondensation of L‐lactic acid to prepare poly(L‐lactic acid) (PLLA)/SiO2 nanocomposite was studied. The change in the appearance of the reaction mixture was tracked, and the resultant oligo(L‐lactic acid) (OLLA)/SiO2 and PLLA/SiO2 nanocomposites were characterized by transmission electron...
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