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In this paper, nickel nanofibers were prepared by electrospinning polyvinyl alcohol/nickel nitrate precursor solution followed by high temperature calcination in air and deoxidation in hydrogen atmosphere. The thermal stability of the as-electrospun PVA/Ni(NO 3 ) 2 composite nanofibers were characterized by TG–DSC. The morphologies and structures of the as-prepared samples were characterized...
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