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The far and mid infrared (FIR/MIR) spectra of powdered Os(η5‐C5Me5)2 (OsCp*2) as well as the polarized Raman spectra of an oriented single crystal (where the two molecules of D5h symmetry in the unit cell are uniformly oriented) have been recorded. The latter allow the assignment of the observed Raman lines to irreducible representations (irreps) which agree well with the predictions of a calculation...
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