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Pressureless sintering in vacuum was applied to synthesize Ti 3 SiC 2 from elemental powders of Ti, Si and C. Based on the phase compositions and purities of the products obtained by X-ray diffraction, the elemental powders composition and sintering condition were optimized. It was found that the sample sintered at 1450 o C for 240min from a mixture of 3Ti/1.75Si/2C (molar...
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