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Hydrothermal syntheses at 185 °C for 24 h yield pure cubic Ia$ \bar 3 $ nanocrystalline Tm3+‐doped Lu2O3 materials, whose morphologies are controlled through the conditions of the reaction. Chloride reagents under mild conditions produce rods of ∼15 µm length x 90 nm ∅︁ size. These nanorods exhibit photoluminescence at ∼1.95 µm, and fluorescence lifetime τ = 976 µs has been measured for 3F4 in the...
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