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A radical 11C‐aminocarbonylation protocol characterized by excellent substrate compatibility was developed to transform alkyl iodides into 11C‐labelled amides, including the 11β‐HSD1 inhibitor [carbonyl‐11C]adamantan‐1‐yl(piperidin‐1‐yl)methanone. This protocol serves as a complementary extension of palladium‐mediated 11C‐aminocarbonylation, which is limited to the preparation of 11C‐labelled compounds...
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