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Monodisperse microspheres constructed with rutile TiO2 nanorods were synthesized by a hydrothermal reaction of TiCl3 with Na2C2O4, ethylene glycol (EG) and H2O at 140–220°C for 4–12 h. The diameter of the microspheres can be changed in the range of 190–1200 nm by tuning the reaction temperature and time. The constituent nanorods grow along the c-axis of rutile, the side facets of which are (110),...
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