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Fabrication of a patterned hydrogen‐bonded organic framework (HOF) films on a large scale is an extreme challenge. In this work, a large area HOF film (30 × 30 cm2) is prepared via an efficient and low‐cost electrostatic spray deposition (ESD) approach on the un‐modified conductive substrates directly. Combining the ESD with a template method, variously patterned HOF films can be easily produced,...
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