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Isobutyronitrile has been selected as a stable substitute for the 2‐cyano‐2‐propyl radical originating from 2,2′‐azobis(isobutyronitrile) to study the behavior of this radical in miniemulsion polymerization. The partition of isobutyronitrile between styrene monomers/polymers and water has been investigated by carrying out equilibrium experiments under different conditions. Prediction based on a published...
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