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For overall water‐splitting systems, it is essential to establish O2‐insensitive cathodes that allow cogeneration of H2 and O2. An acid‐tolerant electrocatalyst is described, which employs a Mo‐coating on a metal surface to achieve selective H2 evolution in the presence of O2. In operando X‐ray absorption spectroscopy identified reduced Pt covered with an amorphous molybdenum oxyhydroxide hydrate...
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