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Monodisperse α-Fe2O3 microspheres have been selectively synthesized through a facile hydrothermal method without the assistance of any surfactant, employing FeCl3·6H2O and NH4NaHPO4 as initial materials. The products were characterized by X-ray diffraction, scanning electron microscopy, and transmission electron microscopy. α-Fe2O3 microspheres with average size about 250 nm were constructed by single...
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