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Extraction of an alloy of the nominal composition “KSnBi” by an [18]crown‐6 melt, and subsequent by 1,2‐diaminoethane (en) resulted in the formation of a new ternary Zintl salt [K([18]crown‐6)]2[Sn2Bi2] (1) comprising the known binary anion [Sn2Bi2]2–. Herein we report synthesis and structure of 1, along with a density functional (DFT) study of the anion. The crystal structure of 1 was solved and...
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