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Hip to be square: Tetranuclear metallamacrocycles containing Pd–allyl and either Pd(dppp) or Pt(dppp) moieties (dppp=1,3‐bis(diphenylphosphino)propane) have been obtained from the selective combination of three different building blocks. The study of their unusual dynamic behavior demonstrated the equilibrium between the self‐assembled supramolecules and their components (see scheme).
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