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A novel hybrid material, containing alternating layers of molybdenum oxide covalently bonded to the electron-rich 3,8-phenanthroline as the spacer molecules, has recently been realised. The structure of [MoO3(3,8-phenanthroline)0.5] consists of corner-shared {MoO5N} octahedra where the Raman spectra correlate very well with the structural data. It is demonstrated here that the choice of the ligands...
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