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The electrochemical reduction of tert-butyl hydroperoxide has been investigated in dimethylformamide and 1,2-dichloroethane. Voltammograms at platinum or at glassy carbon electrodes were indistinguishable from the background, whereas at iron electrodes a well-defined cathodic peak was observed. The electrocatalytic reduction of tert-butyl hydroperoxide was enhanced at freshly electrodeposited iron...
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