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While reaction of [η5-RC5H4(CO)3Mo]2, PhC≡CPh and Cp2Ni yields Mo/Ni hetero- and Mo/Mo homobimetallic complexes [η5-RC5H4(CO)2MoNiCp](μ-C2Ph2) [(1a) R = MeCO; (1b) R = MeO2C] and [η5-RC5H4(CO)2Mo]2(μ-C2Ph2) [(2a) R = MeCO; (2b) R = MeO2C], reaction of [η5-RC5H4(CO)3W]2, PhC≡CPh and Cp2Ni give W/Ni heterobimetallic compounds [η5-RC5H4(CO)2WNiCp](μ-C2Ph2) [(3a) R = MeCO; (3b) R = EtO2C] without an appreciable...
The isolobal reaction of the tetrahedral cluster Ph2C2Co2(CO)6with η5-CHOC5H4(CO)3MNa (M = Mo, W) yields η5-CHOC5H4MCoC2Ph2(CO)5 [(1) M = Mo, (2) M = W], whereas M–M singly-bonded dimers [η5-RC5H4- M(CO)3]2 [M = Mo, R = Ac; M = Mo, W, R = CHO] react with Co2(CO)8 to give η5-AcC5H4MoCo3(CO)11(7) and η5-C5H5MCo3(CO)11 [(8) M = Mo, (9) M = W], respectively. While (1) and (2) react with 2,4-dinitrophenylhydrazine...
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