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Five nitrogen sources (glycine, β‐alanine, urea, melamine and nicotinamide) and three heating methods (thermal, monomodal microwave and multimodal microwave) are used to prepare nitrogen‐doped Starbons® derived from starch. The materials are initially produced at 250–300 °C (SNx300y), then heated in vacuo to 800 °C to produce nitrogen‐doped SNx800y’s. Melamine gives the highest nitrogen incorporation...