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4‐Aminophenylmethylphosphonic acid was grafted on ITO surfaces by 1) electrochemical reductive adsorption of the corresponding aryl diazonium salt and 2) by self‐assembly via the phosphonic acid moiety. The aryl diazonium salt derived surfaces are reasonably stable within a wide potential range from −600 mV to 600 mV compared to a very narrow stable range between −40 mV and 40 mV for the self‐assembled...
In situ generated aryl diazonium cations were synthesized in the electrochemical cell by reaction of the corresponding amines with NaNO2 in aqueous HCl. This paper reports a study of the formation of mixed layers from in situ generated aryl diazonium cations. Firstly, glassy carbon (GC) and gold electrode surfaces were modified with five single in situ generated aryl diazonium salts to obtain their...
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