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The aim of the present study was elucidating reaction mechanism of the TiO2–Al–C–Fe system during self-propagating high-temperature synthesis. Results showed that the addition of Fe to the 3TiO2+4Al+3C reactants from 1.21mol to 1.71mol led to instability of the combustion reaction and the formation of nano-crystalline TiC. Differential thermal analysis and X-ray diffraction analysis results demonstrated...
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