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Solution-based combinatorial samples of lithium manganese nickel oxide were synthesized and studied by X-ray diffraction in order to map out the pseudo-ternary system over the entire metal composition ranges. More than 300 compositions were prepared and many duplicates were made to test reproducibility. The samples were made by heating to 800°C in an oxygen atmosphere and two cooling methods were...
Solution based combinatorial samples of lithium nickel oxide were synthesized and studied by X-ray diffraction in order to develop a method that limits the amount of lithium lost during synthesis. Variables tested were the substrate used (alumina, magnesia or alumina treated with LiOH), heating temperature, the atmosphere during heating (air or oxygen) and the chemical used to precipitate the metals...
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