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The electrodeposition processes of nickel in ammonium chloride media were studied in combination of speciation analysis and in situ synchrotron radiation X-ray imaging. The X-ray absorption spectra indicated that the nickel(II) species present an octahedral configuration independent on aqueous pH. The UV–vis spectra and fraction-pH diagram showed that the dominant species is Ni(H2O)62+, Ni(NH3)m(H...
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