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We have studied the molecular dynamics of one of the major macromolecules in articular cartilage, chondroitin sulfate. Applying 13C high‐resolution magic‐angle spinning NMR techniques, the NMR signals of all rigid macromolecules in cartilage can be suppressed, allowing the exclusive detection of the highly mobile chondroitin sulfate. The technique is also used to detect the chondroitin sulfate in...
The surface dynamics of bacteriorhodopsin was examined by measurements of site-specific 13C1H dipolar couplings in [3-13C]Ala-labeled bacteriorhodopsin. Motions of slow or intermediate frequency (correlation time 50s) scale down 13C1H dipolar couplings according to the motional amplitude. The two-dimensional dipolar and chemical shift (DIPSHIFT) correlation technique was utilized to obtain the dipolar...
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