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High crystalline cerium hexaboride (CeB6) nanoparticles (NPs) were synthesized using mixture of mag‐ nesium (Mg), cerium oxide (CeO2) and boron oxide (B2O3) via the mechanochemical process at room tem‐ perature. Based on the results, magnesiothermic reduction of B2O3 occurred after about 2 h of milling in a mechanically induced self‐sustaining reaction (MSR). The significant amount of heat produced...
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