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The synthesis of Ni(II) and Pd (II) coordination complexes containing Schiff's bases derived from the condensation of 2,4‐dihydroxybenzaldehyde with 4‐chloroaniline (L1) or 3,5‐dichloroaniline (L2) is described. The condensation of ligands L1 and L2 with chlorodiisopropylphosphine in the presence of a base produced the corresponding non‐symmetric pincer ligands POCOP‐1 and POCOP‐2 with the unexpected...
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