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This paper describes the cathodic electrodeposition of nickel hydroxides from NiCl2 at constant potentials. In a single-compartment electrochemical cell, the procedure yields black films that have the appearance of glassy carbon. XPS analyses reveal that the films consist of a mixture of Ni(OH)2 and NiOOH in a proportion that depends on the deposition potential; furthermore, SIMS analyses indicate...
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