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Anhydrous ytterbium chloride was obtained via solid-phase reaction from Yb2O3 with AlCl3 as a chlorination agent. The electrochemical behavior of the chloridized Yb2O3 was investigated on W electrodes in LiCl–KCl and LiCl–KCl–AlCl3 melts by cyclic voltammetry and square wave voltammetry. The results showed that the reduction/reoxidation of Yb(III)/Yb(II) was reversible and controlled by diffusion...
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