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A rapid method for Pd-promoted cross-coupling of methyl iodide and tributyltin derivatives of tolylisocarbacyclins was developed with the objective of applying to the PET study on the IP 2 receptor in a living human brain. The high efficiency is obtainable for both of the one-pot operation using a large excess of CuCl and the stepwise operation consisting of the initial preparation of a methylpalladium...
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