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In situ attenuated total reflection infrared spectroscopy (ATR-IR) in the liquid phase and in situ transmission IR spectroscopy in the gas phase were used to validate a previously proposed mechanism for limonene epoxidation with aqueous hydrogen peroxide on PW-Amberlite. Catalyst activation by the oxidant was evidenced by ATR-IR through the presence of multiple bands in the 1220–910cm −1 range,...
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