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The continuous and highly intergrown anatase-free TS-1 film was fabricated with TiCl 3 as the titanium source for the first time. The in situ nucleation and secondary growth method was employed to synthesize the TS-1 film. By means of scanning electron microscopy (SEM) images, X-ray diffraction (XRD) patterns, and FT-IR and UV–vis spectra measurements, the resulting film was observed to be...
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