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Mullite and mullite/Y-ZrO 2 (25 and 50vol.%) beads were produced by thermal spraying in water the corresponding atomised compositions. The amount of amorphous phases in the as-sprayed beads was comparatively determined by X-ray diffraction (XRD) and differential thermal analysis (DTA) methods. Characteristic XRD peaks associated to crystallization of the mullite and Y-ZrO 2 (t) phases...
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