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The results of MoS2/carbon nanocomposite hydrothermal synthesis is presented. The synthesized material was studied by XRD, TEM, EDS, SAXS, and porosimetry. The multilayer nanospheres with the average size 40–70 nm were obtained. The investigations confirm the formation of particles with double‐hierarchical structure where 2H‐MoS2 layers alternate with carbon layers. Atomic ratio of MoS2:C is about...
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