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One-step solvothermal method has been proved to be a simple and efficient route to synthesize three-dimensional (3D) hierarchical TiO2 microsphere structures, but discrepant properties of the solvent media had been claimed as the major factors determining microstructures and properties of the final products. In this study, several typical solvents, including alkane, aromatic hydrocarbons, halohydrocarbon,...
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