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An efficient and rapid (10–20min) one-pot synthesis of chemically and pharmaceutically interesting 1,4-oxathian-2-ones is reported. The protocol involves LiBr catalyzed regioselective ring-opening–ring-closing reaction cascade of terminal epoxides with α-mercaptocarboxylic acids at rt under solvent-free conditions. Recycling of the catalyst, atom economy, and formation of water as the only by-product...
The first example of one-pot oxidative anti-Markownikov bromohydroxylation and bromoalkoxylation of Baylis–Hillman (BH) adducts (olefins) is reported. The reaction is performed at rt using LiBr as the bromine source and 2-iodoxybenzoic acid (IBX) as the oxidant. The process involves oxidation of BH adducts with IBX to give β-ketomethylene compounds in situ, which undergo highly regioselective vicinal...
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