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Synthesis experiments in the system Li2O–CaO–SiO2 resulted in the formation of single-crystals of Li2Ca2Si2O7. Structural investigations were based on single-crystal diffraction. At ambient conditions the compound has the following basic crystallographic data: hexagonal symmetry, space group P6122, a=5.0961(2)Å, c=41.264(2)Å, V=928.07(6)Å3, Z=6. Structure solution was performed using direct methods...
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