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Hexagonal tris(o‐phenylenedioxy)cyclotriphosphazene (TPP) is used as ahost for organizing dipolar molecular rotor guests into regular trigonal arrays. Inclusion of molecular rotors with transversely dipolar rotators into TPP channels is followed by solid‐state nuclear magnetic resonance, diifferential scanning calorimetry, X‐ray diffraction, and dielectric spectroscopy. The more polar of the two rotors...
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