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A series of spinel oxy-fluorides with the formula LiMn 1.8 Li 0.1 Ni 0.1 O 4−η F η have been synthesized by both the conventional high-temperature (800 °C) firing method with LiF and a low temperature (450 °C) firing process with NH 4 HF 2 . Interestingly, the samples obtained by the high temperature (800 °C) procedure show no fluorine in the...
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