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A new Li-Ni-Mn spinel of the composition Li0.5Ni0.5Mn2O4 was successfully prepared by thermal decomposition of citrate complexes followed by quenching from 1048 K. The distribution of cations in this oxide was deduced from X-ray powder diffraction and XPS measurements. High pressure powder X-ray diffraction measurements were performed up to pressures of approximately 6 GPa. The cubic spinel phase...
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