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One-pot syntheses of new water-soluble dicobalt complexes having two cobalt carbon bonds are reported. The complexes were characterized by 1 H NMR and UV-vis spectroscopies as well as ESI-MS. These complexes were photosensitive, and photo-cleavage of the cobalt carbon bonds upon irradiation with visible light produced methyl radicals which were detected by ESR spin-trapping techniques. The...
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