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Single‐atom‐layer catalysts with fully activated basal‐atoms will provide a solution to the low loading‐density bottleneck of single‐atom catalysts. Herein, we activate the majority of the basal sites of monolayer MoS2, by doping Co ions to induce long‐range ferromagnetic order. This strategy, as revealed by in situ synchrotron radiation microscopic infrared spectroscopy and electrochemical measurements,...
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